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反響硫酸濃度的斷定質料硫酸的濃度和反響時稀釋的濃度斷定對酸解反響的好壞有顯著的影響。前面已說到理論上質料硫酸的濃度從85%到98%都能夠運用，但運用92.5%~95%的硫酸為好，因為質料硫酸濃度過高(＞96%)不只在稀釋時會放出更多的熱量，并且高濃度的硫酸中H+和SO42-濃度高、活性大使反響速度加速，而質料硫酸濃度過低(＜92%)因為稀釋熱較少，酸解反響陡峭、固相物緊實不易浸取、安穩性差。

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